Modification History
Not applicable.
Unit Descriptor
Unit descriptor |
This unit of competency covers the ability to analyse samples using specialist techniques and modern accessories that extend the capability of fourier transform infra red (IR or FTIR) spectrometers. The unit includes establishing client needs for routine and non-routine samples, optimising enterprise procedures and instruments for specific samples, obtaining valid and reliable data and reporting test results. Personnel are required to recognise atypical test data/results and troubleshoot common analytical instrument and procedure problems and perform routine instrument maintenance. |
Application of the Unit
Application of the unit |
This unit of competency is applicable to experienced laboratory technical officers/technicians, laboratory supervisors and technical specialists who conduct instrumental analysis in laboratories providing consultancy, research and development and quality assurance services. These services may be provided for a wide range of industry sectors, such as biomedical (e.g. bacterial screening), forensic science (e.g. fingermark residues, paints and fibres), environmental monitoring (pollutants in air, soil and water), industrial analysis (textile fibres, polymers, lubricant condition, defect and surface contamination), pharmaceutical products (drug analysis) and food (e.g. nutrition supplement analysis). Industry representatives have provided case studies to illustrate the practical application of this unit of competency and to show its relevance in a workplace setting, at the end of this unit of competency under the section This competency in practice. |
Licensing/Regulatory Information
Not applicable.
Pre-Requisites
Prerequisite units |
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Employability Skills Information
Employability skills |
This unit contains employability skills. |
Elements and Performance Criteria Pre-Content
Elements describe the essential outcomes of a unit of competency. |
Performance criteria describe the performance needed to demonstrate achievement of the element. Where bold italicised text is used, further information is detailed in the required skills and knowledge section and the range statement. Assessment of performance is to be consistent with the evidence guide. |
Elements and Performance Criteria
ELEMENT |
PERFORMANCE CRITERIA |
1. Determine sample characteristics and appropriate analytical methods |
1.1. Interpret client request and/or perform presumptive tests to identify sample characteristics and determine the most appropriate IR spectroscopic technique 1.2. Liaise with client or sample provider to review client needs, testing requirements and sample history, if necessary 1.3. Identify analytical standards, reference materials, test methods and enterprise procedures that may be applicable 1.4. Select the most appropriate standard test method that is consistent with testing requirements and instrument availability 1.5. If no standard method exists, adapt or modify a test method to suit the sample characteristics 1.6. If necessary, seek advice from supervisor about any proposed variations and document all approved changes to test methods 1.7. Schedule analysis using enterprise procedures |
2. Prepare samples and standards |
2.1. Log sample into instrument software 2.2. Obtain a representative analytical portion of the laboratory sample 2.3. Prepare sample in accordance with selected test method 2.4. Prepare validation checks and/or calibration standards for analytical portions |
3. Set up instrument and perform trial analysis |
3.1. Configure the appropriate instrument accessories to perform the selected test method 3.2. Perform other pre-use, calibration and safety checks using enterprise procedures 3.3. Set instrumental parameters in accordance with those specified in selected test method 3.4. Check and optimise each instrument sub-system 3.5. Conduct performance tests using standards and samples 3.6. Assess instrument performance in terms of response, resolution and number of scans required |
4. Optimise instrument performance |
4.1. Adjust instrumental parameters in a logical and efficient sequence to optimise performance 4.2. When optimisation is achieved, check that the detector and system software can correctly identify and quantify the required species |
5. Perform analysis |
5.1. Measure analyte response for standards, validation checks and samples using optimised instrument settings 5.2. Conduct sufficient measurements to obtain reliable data 5.3. Use system software to produce calibration graphs, spectra, confirm data quality and calculate uncertainties 5.4. Check that results are consistent with estimations and expectations 5.5. Analyse trends in data and/or results and report out of specification or atypical results promptly to appropriate personnel 5.6. Return instrument to standby or shutdown condition in accordance with enterprise procedures 5.7. Report results with the appropriate accuracy, precision, uncertainty and units |
6. Perform routine maintenance and troubleshoot instruments |
6.1. Regularly check the spectral and photometric performance of the instrument 6.2. Regularly clean sample cell and/or reflectance crystal faces and replace consumables as appropriate 6.3. Confirm optical matching for cell pairs as necessary 6.4. Identify the need for repairs or servicing and determine whether local repair/maintenance is technically possible and economic 6.5. Arrange for repair or servicing from an accredited agent or other appropriate personnel in accordance with enterprise procedures |
7. Maintain a safe work environment |
7.1. Identify risks, hazards, safety equipment and control measures associated with sample handling/preparation and test method 7.2. Use personal protective equipment and safety procedures specified for test method and materials to be tested 7.3. Minimise the generation of wastes and environmental impacts 7.4. Ensure the safe collection/disposal of laboratory wastes 7.5. Clean, care for and store equipment and consumables in accordance with enterprise procedures |
8. Maintain laboratory records |
8.1. Enter approved data and results into laboratory information management system (LIMS) 8.2. Maintain logs of instrument calibration checks, use and maintenance in accordance with enterprise procedures 8.3. Maintain security, integrity and traceability of samples, results and documentation 8.4. Communicate results to appropriate personnel in accordance with enterprise procedures |
Required Skills and Knowledge
REQUIRED SKILLS AND KNOWLEDGE |
This section describes the skills and knowledge required for this unit. |
Required skills |
Required skills include:
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Required knowledge |
Required knowledge includes:
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Evidence Guide
EVIDENCE GUIDE |
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The Evidence Guide provides advice on assessment and must be read in conjunction with the performance criteria, required skills and knowledge, range statement and the Assessment Guidelines for the Training Package. |
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Overview of assessment |
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Critical aspects for assessment and evidence required to demonstrate competency in this unit |
Assessors should ensure that candidates can:
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Context of and specific resources for assessment |
This unit of competency is to be assessed in the workplace or simulated workplace environment. This unit of competency may be assessed with:
Resources may include:
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Method of assessment |
The following assessment methods are suggested:
In all cases, practical assessment should be supported by questions to assess underpinning knowledge and those aspects of competency which are difficult to assess directly. Where applicable, reasonable adjustment must be made to work environments and training situations to accommodate ethnicity, age, gender, demographics and disability. Access must be provided to appropriate learning and/or assessment support when required. The language, literacy and numeracy demands of assessment should not be greater than those required to undertake the unit of competency in a work like environment. |
This competency in practice |
Industry representatives have provided the case studies below to illustrate the practical application of this unit of competency and to show its relevance in a workplace setting. Forensic science A forensic science team is examining some motor vehicle paint samples taken from a crime scene. After a careful microscopic examination of the topcoat and undercoat layers, one technician narrows the sample's origin down to a small range of possible vehicle makes, models and years of manufacture. To aid identification, another technician prepares a small paint chip for examination in the laboratory's FTIR spectrometer. After referring to the recommended analytical methods, he/she decides to use a transmittance technique because all the sampling wavelengths are subjected to the same path lengths and most of the reference data for paints, binders, pigments and additives consist of transmittance spectra. The technician cuts a cross-section sample with a microtome to expose an edge of the multi-layered sample and then mounts it using the microscope accessory. He/she adjusts the microscope aperture to minimise stray light and diffraction effects before obtaining spectra for each layer. After comparing his/her results with the spectral library data for binders, pigments and additives used by the manufacturers of interest, the origin of the paint is identified. Some weeks later, confirmation is obtained when samples taken from a suspect's vehicle match the physical and chemical features and spectra determined from the crime scene samples and diffuse reflectance measurements on the two sets of samples show identical weathering and surface contamination. |
Range Statement
RANGE STATEMENT |
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The range statement relates to the unit of competency as a whole. It allows for different work environments and situations that may affect performance. Bold italicised wording, if used in the performance criteria, is detailed below. Essential operating conditions that may be present with training and assessment (depending on the work situation, needs of the candidate, accessibility of the item, and local industry and regional contexts) may also be included. |
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Codes of practice |
Where reference is made to industry codes of practice, and/or Australian/international standards, it is expected the latest version will be used |
Standards , codes , procedures and /or enterprise requirements |
Standards, codes, procedures and/or enterprise requirements may include:
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IR /FTIR instruments and techniques |
IR/FTIR instruments and techniques may include:
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Testing that uses IR /FTIR spectroscopy |
Testing that uses IR/FTIR spectroscopy may include:
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Presumptive tests |
Presumptive tests may include:
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Sample and standard preparation |
Sample and standard preparation may include:
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Pre-use , calibration and safety checks |
Pre-use, calibration and safety checks may include:
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Instrumental parameters |
Instrumental parameters may include:
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Common analytical procedure problems and remedies |
Common analytical procedure problems and remedies may include:
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Common equipment problems |
Common equipment problems may include:
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Hazards |
Hazards may include:
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Addressing hazards |
Addressing hazards may include:
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Occupational health and safety (OHS ) and environmental management requirements |
OHS and environmental management requirements:
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Unit Sector(s)
Unit sector |
Testing |
Competency field
Competency field |
Co-requisite units
Co-requisite units |
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